CHEM 260: Synthetic Chemistry Laboratory
Course Goals
To learn new techniques as applied to problems in the synthetic chemistry laboratory. Many of the techniques will be new and build on the basic lab skills acquired in first year. These include reflux, distillation, recrystallization, inert atmosphere reactions, chromatography, rotary evaporation, and how to work safely in a fumehood. These techniques build a foundation for the upper-level laboratory synthesis courses, Chem 362 & 363.
To understand the relationship between a compound’s structure, physical properties, and the spectra observed for the compound. The physical properties of a compound can indicate if the correct product was isolated or not, as well as comment on the purity. Spectroscopic analysis (primarily IR & NMR) is paramount in determining the structure of small molecules. A variety of classes of organic and inorganic compounds are synthesized in the laboratory, and their structures can be understood in terms of their spectra. Additional techniques of analysis will include magnetic susceptibility, polarimetry, UV-Vis spectroscopy, gas chromatography, and mass spectrometry.
To gain self-confidence in a laboratory setting. Students are responsible for planning their time in the laboratory in order to complete the work on schedule. Preparation is key.